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ENVIRONMENTAL ANALYSES (*Indicates NELAP Certified Analysis)
SOIL AND WATER
Acidity – EPA 305.1 or SM 2310
Alkalinity – EPA 310.1 or SM 2320B
*Base/Neutral & Acid Extractables
GC/MS Analysis of Semi-Volatile Organics, EPA 625 or EPA 8270
*Biological Oxygen Demand (BOD) – EPA 405.1
*Chemical Oxygen Demand (COD) – EPA 410.4
*Chlorinated Herbicides – EPA 615 or EPA 8151
Chlorinated Hydrocarbons – EPA 612 or EPA 8121
Chlorine, Total Residual – EPA 330.5
Coliform (Total & Fecal) – SM 9221, SM 9221 Modified, SM 9222, SM 9222 Modified
Color – EPA110.2 or SM 2120B
*Conductivity (Specific Conductance) – EPA 120.1
*Cyanide, Amenable to Cl- -- EPA 335.4 or EPA 9012
*Cyanide, Total – EPA 335.4 OR EPA 9012
Cyanide, Available – OIA 1667
Diesel Range Organics (DRO) – EPA 8015M or 8270M
Extractable Organic Halides (EOX) – EPA 9023
*Flashpoint (Ignitibility) – EPA 1010
Formaldehyde – EPA 8315
Gasoline Range Organics (GRO) – EPA 8015M or EPA 8260
Glycols – EPA 8015M
*Hardness (by calculation) – SM 2340B
Hexavalent Chromium (Cr-VI) –(EPA 3060/7195-Prep Methods) Analyzed by EPA 6010.
*Ion Chromatography – EPA 300.0
Including Chloride, Fluoride, Nitrate, Nitrite, Sulfate
Metals –
Inductively Coupled Plasma (ICP) – EPA 200.7 or EPA 6010.
*ICP-Mass Spectroscopy – EPA 200.8 or EPA 6020.
Metals Scan:
Aluminum (Al), Antimony (Sb), Arsenic (As), Barium (Ba), Beryllium (Be), Boron (B), Cadmium (Cd), Calcium (Ca), Chromium (Cr), Cobalt (Co), Copper (Cu), Iron (Fe), Lead (Pb), Lithium (Li), Magnesium (Mg), Manganese (Mn), Molybdenum (Mo), Nickel (Ni), Potassium (K), Selenium (Se), Silver (Ag), Sodium (Na), Strontium (Sr), Thallium (Tl), Tin (Sn), Titanium (Ti), Vanadium (V), and Zinc (Zn).
10 Michigan Metals: Arsenic, Barium, Cadmium, Chromium, Copper, Lead, Mercury,
(DEQ, MDNR) Selenium, Silver, Zinc.
RCRA Metals: Arsenic, Barium, Cadmium, Chromium, Lead, Mercury, Selenium, Silver.
Priority Pollutant Metals: Antimony, Arsenic, Beryllium, Cadmium, Chromium, Copper, Lead, Mercury, Nickel, Selenium, Silver, Thallium, and Zinc.
*Mercury – (Hg) EPA 245.1 or EPA 7470 or EPA 7471
Mercury(low level) - (Hg) EPA 1631
Methylene Blue Active Substances (MBAS - Surfactants) – EPA 425.1
*Nitrogen, Kjeldahl – EPA 351.2
*Nitrogen, Ammonia – EPA 350.3
*Nitrogen, Nitrate (NO3) – EPA 300.0
*Nitrogen, Nitrite (NO2) – EPA 300.0
Odor Threshold – EPA 140.1
Oil & Grease, Total Recoverable – EPA 413.1 or EPA 1664 (Gravimetric)
EPA 418.1 (Infrared)
*Organochlorine Pesticides – EPA 608 or EPA 8081
Organophosphorus Herbicides – EPA 8141
Paint Filter Test – EPA 9095
Percent Solid – ASTM D 2216
Percent Water – Karl Fischer Titration – ASTM E 203
Moisture Content – ASTM D 2216
*pH (Corrosivity) – EPA 150.1
Phenols – EPA 604 or 624 or 8270 or 8041
*Phenolics, Total – EPA 420.2
*Phosphorus, All Forms – EPA 365.2
Phthalate Esters – EPA 606 or EPA 624 or EPA 8270 or EPA 8061
*Polychlorinated Biphenyls (PCBs) – EPA 608 or EPA 8082
*Polynuclear Aromatic Hydrocarbons (PAHs) – EPA 625 or EPA 8270
Reactivity --
Cyanide – EPA SW846 Sect. 7.3.3.2 or EPA 9010
Sulfide – EPA SW846 Sect. 7.3.4.2 or EPA 9030
Solids – Residue
Filterable (Total Dissolved Solids) – EPA 160.1 or SM 2540C
Non- filterable (Total Suspended Solids) – EPA 160.2
Settleable – SM 2540
Total (Percent Solid) – EPA 160.3 or ASTM D-2216
Volatile Solids – EPA 160.4 or SM 2540E
Specific Gravity – ASTM D-70
Sulfide – EPA 376.1 or EPA 9030
Sulfite – EPA 377.1
Temperature (field parameter) – EPA 170.1
*Total Organic Carbon (TOC) – EPA 415.1 or EPA 9060
Total Organic Halide (TOX) – EPA 9020
Total Petroleum Hydrocarbons (TPH) – EPA 418.1 or EPA 8015M or EPA 8100
Turbidity – EPA 180.1
Volatile Organics --
*Purgeable Aromatics – EPA 602 or EPA 8020 or EPA 8260 (* Mass Spectrometry Only)
*Purgeable Halocarbons - EPA 8260
*Purgeable Organics – EPA 8260
Purgeable Petroleum Hydrocarbons – EPA 8015M WASTE CHARACTERIZATION
State Regulated Parameters
Michigan Department of Environmental Quality
Organics
Volatile Organics – EPA 8260
Semi-Volatile Organics – EPA 8270
Polynuclear Aromatic Hydrocarbons (PAHs or PNAs) – EPA 8270 or EPA 8310
Organochlorine Pesticides – EPA 8081
Polychlorinated Biphenyls (PCBs) – EPA 8082
Inorganics - 10 Michigan Metals:(DEQ, MDNR) Arsenic, Barium, Cadmium,
Chromium, Copper, Lead, Mercury, Selenium, Silver, Zinc.
· Inductively Coupled Plasma (EPA 200.7) and/or ICP-Mass Spectroscopy (EPA 200.8)
Mercury – EPA 7470 or EPA 7471
Federal Regulated Parameters
Toxicity Characteristic Leaching Procedure (TCLP) – EPA 1311 or Synthetic Precipitation Leaching Procedure (SPLP) – EPA 1312
Volatile Organics – Benzene, Carbon tetrachloride, Chlorobenzene, Chloroform, 1,2-Dichloroethane, 1,1-Dichloroethene, Methyl ethyl ketone (MEK), Tetrachloroethene, Trichloroethene, Vinyl chloride.
Semi-Volatile Organics – Cresols (o-, m-, & p-Methylphenol), 1,4-Dichlorobenzene, 2,4-Dinitrotoluene, Hexachlorobenzene, Hexachlorobutadiene, Hexachloroethante, Nitrobenzene, Pentachlorophenol, Pyridine, 2,4,5-Trichlorophenol, 2,4,6-Trichlorophenol.
Pesticides – Chlordane, Endrin, Heptachlor, Heptachlor epoxide, Lindane, Methoxychlor, Toxaphene.
Herbicides – 2,4-D and Silvex (2,4,5-TP).
Metals – Arsenic, Barium, Cadmium, Chromium, Copper, Lead, Mercury, Selenium, Silver, Zinc.
Corrosivity (pH) – EPA 150.1
Ignitibility (Flashpoint) – EPA 1010
Reactivity—
Cyanide – EPA SW846 Sect. 7.3.3.2 or EPA 9010
Sulfide – EPA SW846 Sect. 7.3.4.2 or EPA 9030
DRINKING WATER
Volatile Organic Compounds – EPA 524.2
Trihalomethanes – EPA 524.2 Bromoform, Chloroform, Bromodichloromethane, Chlorodibromomethane
EDB (Ethylene dibromide) and DBCP (1,2-Dibromo-3-chloropropane)– EPA 504.1
Chlorinated Pesticides – EPA 508 – Aldrin, Chlordane, Dieldrin, Endrin, Heptachlor, Heptachlor epoxide, Hexachlorobenzene, Hexachlorocyclopentadiene, Lindane (gamma-BHC), Methoxychlor, Propachlor, Toxaphene, Trifluralin. (Subcontracted to State Lab)
PCBs as Decachlorobiphenyl – EPA 508A (Subcontracted to State Lab)
Chlorinated Herbicides – EPA 515.1 – 2,4-D, Silvex (2,4,5-TP), 2,4,5-T, Dalapon, Dinoseb, Dicamba, Pentachlorophenol, Picloram, Aciflurofen. (Subcontracted to State Lab)
Coliforms (Total & E.coli) – SM 9223
Organophosphorus Pesticides – EPA 507 – Atrazine, Alachlor, Simazine (Subcontracted to State Lab)
Metals – EPA 200.8 – Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Chromium, Copper, Lead, Manganese, Molybdenum, Nickel, Selenium, Thallium, Zinc.
Mercury – EPA 245.1
Inorganics
Alkalinity – SM 2320B
Chloride, Fluoride, Nitrate, Nitrite, Sulfate – EPA 300.0
Conductivity (Specific Conductance) – EPA 120.1
Hardness – EPA 130.2
pH – EPA 150.1
Total Cyanide – EPA 335.4
Total Organic Carbon – EPA 415.1
